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- W3211944170 abstract "Methoxybenzene-linked polyimides were synthesized by a trifluoromethanesulfonic acid (TfOH)-catalyzed 1,4-addition (Michael addition) reaction. Newly synthesized 1,3-bis(3,5-dimethoxyphenoxy)propane and known 5,5′-oxybis(1,3-dimethoxybenzene) as nucleophilic monomers were reacted with several bismaleimides in the presence of a catalytic amount of TfOH in m-cresol. Use of 1,3-bis(3,5-dimethoxyphenoxy)propane afforded polyimides with number average molecular weights (Mn)s of 8000–15000. However, polyimides with Mn of 4000 or less were obtained when 5,5′-oxybis(1,3-dimethoxybenzene) was employed as a monomer. The synthesized polyimides showed good thermostability as judged by 10% weight loss temperatures between 417 and 441 °C. Their glass transition temperatures were around 200 °C. These polymers featured a wide range of solubility in organic solvents such as m-cresol, DMF, pyridine, and chloroform." @default.
- W3211944170 created "2021-11-22" @default.
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- W3211944170 date "2022-01-01" @default.
- W3211944170 modified "2023-10-14" @default.
- W3211944170 title "Synthesis and characterization of methoxybenzene-linked polyimides formed by 1,4-addition to bismaleimides" @default.
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- W3211944170 doi "https://doi.org/10.1016/j.polymer.2021.124326" @default.
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