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• W3212190895 endingPage "18472" @default.
• W3212190895 startingPage "18466" @default.
• W3212190895 abstract "Improved methods for the synthesis of KB3H8, NH3B3H7, and N-alkyl analogues of NH3B3H7 have been developed based on previous works. KB3H8 was synthesized by the reaction of metallic potassium (K) with borane dimethyl sulfide ((CH3)2S·BH3) with high yield and atom-economy. In the preparation of NH3B3H7 and its N-alkyl analogues, KB3H8 served as a starting material and was converted to THF·B3H7 first through reactions with HCl diethyl ether solution or oxidation agent CoCl2. Then, the formed THF·B3H7 in situ reacted with the corresponding ammonia or amines to form the amine borane final products. This work paves an alternative way for preparing organic-inorganic hybrid materials containing B, N, and C atoms." @default.
• W3212190895 created "2021-11-22" @default.
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• W3212190895 date "2021-11-18" @default.
• W3212190895 modified "2023-10-18" @default.
• W3212190895 title "Improved Methods for the Synthesis of KB₃H₈, NH₃B₃H₇, and <i>N</i>-Alkyl Analogues of NH₃B₃H₇" @default.
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• W3212190895 doi "https://doi.org/10.1021/acs.inorgchem.1c03037" @default.
• W3212190895 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/34793150" @default.
• W3212190895 hasPublicationYear "2021" @default.
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