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- W3212471520 endingPage "105103" @default.
- W3212471520 startingPage "105103" @default.
- W3212471520 abstract "With the increasing demand of industry, the fabrication of single-component epoxy (EP) systems with satisfactory flame retardancy and thermal stability is of great significance. Herein, a novel phosphorus/nitrogen-containing single-component EP (EP/DOPO/BDM/BICP) system was synthesized via incorporating N,N′-bismaleimide-4,4′-diphenylmethane (BDM), benzimidazolyl-substituted cyclotriphosphazene (BICP) and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) into EP. In our previous work, we found that DOPO could promote the decomposition of BICP to produce dissociative benzimidazoles under heating, which endowed the as-fabricated epoxy thermoset with rapid curing speed. However, the addition of DOPO reduced the glass transition temperature (Tg) of epoxy thermosets. To deal with this problem, bismaleimide with superior heat resistance was added. The results indicated that the addition of BDM improved the thermal stability, flame retardancy and smoke suppression of EP/DOPO/BDM/BICP. The obtained thermoset exhibited UL94 V-0 rating, limiting oxygen index (LOI) of 40.5% and low total smoke production (TSP) of 10.4 m2 due to the synergetic flame-retardant effect of phosphaphenanthrene, polybismaleimide and cyclotriphosphazene. This research offers a viable approach to develop single-component EPs with improved flame retardancy, thermal stability and rapid-curing ability." @default.
- W3212471520 created "2021-11-22" @default.
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- W3212471520 date "2022-01-01" @default.
- W3212471520 modified "2023-10-18" @default.
- W3212471520 title "Facile fabrication of single-component flame-retardant epoxy resin with rapid curing capacity and satisfied thermal resistance" @default.
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- W3212471520 doi "https://doi.org/10.1016/j.reactfunctpolym.2021.105103" @default.
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