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• W3214716625 abstract "Neutron reflectometry (NR) has been utilized to study the electric double layer (EDL) of ionic liquids (ILs), however, further improvement of the sensitivity toward interfacial structure would be desirable. We recently proposed two ways to improve the NR sensitivity toward the EDL structure at the IL/electrode interface (J. Phys. Chem. C, 123 (2019) 9223). First, as the electrode, a thin film of metal (Nb) was used with the scattering length density (SLD) and thickness controlled to sensitively analyze the potential dependent EDL structure. Second, the IL cation and anion were chosen so that they have large size and large SLD difference, both of which also increase the sensitivity. In the present study, we have further explored this rational material design for the sensitivity enhancement, by changing the film metal from Nb to Bi whose SLD is closer to those for two bulk materials: Si and the IL used, trihexyltetradecylphosphonium bis(nonafluorobutanesulfonyl)amide. We successfully observed not only the first ionic layer in the EDL but also the overlayers, revealing that the IL cation is specifically adsorbed on the electrode and that the cation-rich first layer induces overscreening in the overlayers up to the third ionic layer. The interfacial structure of ionic liquid (IL) on an electrode was studied using neutron reflectometry. A rational material design of the electrode metal film and IL enabled us to observe not only the first ionic layer but also the overlayers. Quantitative analysis revealed the specific adsorption of IL cation on the electrode which induces overscreening in the overlayers." @default.
• W3214716625 created "2021-11-22" @default.
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• W3214716625 date "2021-12-15" @default.
• W3214716625 modified "2023-10-14" @default.
• W3214716625 title "Overscreening Induced by Ionic Adsorption at the Ionic Liquid/Electrode Interface Detected Using Neutron Reflectometry with a Rational Material Design" @default.
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• W3214716625 doi "https://doi.org/10.1246/bcsj.20210328" @default.
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