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- W3215698499 abstract "General methods have not been previously developed for the synthesis of sterically hindered α-SCF3-substituted carbonyl compounds using nucleophilic trifluoromethylthiolating reagents. Thus, we herein report sp3C-SCF3 bond formation in hindered α-bromoamides containing 3-bromo-oxindoles and linear α-bromoamides using CuSCF3 or AgSCF3 under mild conditions to access sterically hindered α-SCF3-substituted amides. This transformation is applicable to not only 3-SCF3-substituted oxindoles but also primary and secondary amides and reveals a broad functional group tolerance. This method will benefit the fields of medicinal and agricultural chemistry." @default.
- W3215698499 created "2021-12-06" @default.
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- W3215698499 date "2021-12-02" @default.
- W3215698499 modified "2023-10-17" @default.
- W3215698499 title "Trifluoromethylthiolation of Hindered α-Bromoamides with Nucleophilic Trifluoromethylthiolating Reagents" @default.
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- W3215698499 doi "https://doi.org/10.1021/acs.joc.1c02316" @default.
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