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• W3217038801 abstract "Abstract We present a new approach to determine in situ CO 2 and H 2 O concentrations in apatite via attenuated total reflection Fourier transform infrared spectroscopy (ATR-FTIR). Absolute carbon and hydrogen measurements by nuclear reaction analysis (NRA) and elastic recoil detection (ERD) are used to calibrate ATR-FTIR spectra of CO 2 and H 2 O in apatite. We show that CO 2 and H 2 O contents in apatite can be determined via linear equations ( r 2 > 0.99) using the integrated area of CO 2 and H 2 O IR absorption bands. The main benefits of this new approach are that ATR-FTIR analyses are non-destructive and can be conducted on polished sample material surfaces with a spatial resolution of ~ 35 μm. Furthermore, the wavenumber of the phosphate IR absorption band can be used to determine the crystallographic orientation of apatite, which allows for accurate quantification of CO 2 and H 2 O in randomly orientated apatite grains. The limit of quantification of H 2 O in apatite is ~ 400 ppm and ~ 100 ppm for CO 2 . Via two examples, one from a carbonatite and one from a metasedimentary rock, we show that this new technique opens up new possibilities for determining volatile concentrations and behavior in a wide range of hydrothermal, igneous, and metamorphic systems." @default.
• W3217038801 created "2021-12-06" @default.
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• W3217038801 date "2021-11-26" @default.
• W3217038801 modified "2023-10-16" @default.
• W3217038801 title "Measuring in situ CO2 and H2O in apatite via ATR-FTIR" @default.
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• W3217038801 doi "https://doi.org/10.1007/s00410-021-01858-6" @default.
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