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- W3217606906 abstract "• One novel non-interpenetrated two dimensional structure with U-shaped Cu 4 I 4 clusters was constructed. • The synthesis, crystal structure and luminescent properties of the compound were described. • The compound shows high fluorescent quenching efficiency to Fe 3+ ion. A new two-dimensional coordination polymer with formula of Cu 4 I 4 (3-bpcd) 2 ·C 2 H 5 OH·1.5CH 3 CN ( 1 ) (3-bpcd=N,N'-bis(pyridin-3-yl) cyclohexane-1,4-dicarboxamide), has been synthesized at room temperature and structurally characterized. Crystallography study shows that 1 contains Cu 4 I 4 clusters, which geometry significantly different from reported those called “cubane”, “stairstep” and “fliggy octahedron”. The Cu 4 I 4 clusters in the structure of 1 were connected by semi-rigid ligand (3-bpcd) to form a two dimensional layer (4, 4) net, while Cu 4 I 4 clusters are regarded as 4-connected nodes. These layers further stack in an ABAB fashion and each layer connect by hydrogen bond to generate a three dimensional framework. Thermogravimetric analysis reveals that 1 processes high thermal stability up to about 320 °C. Powder X-ray diffraction analysis indicates that the framework of structure of 1 could be stable in water/ethanol. The luminescent properties study of 1 show that the fluorescence intensity decreased with increase of the concentration of metal ions. Further study indicated that 1 could be used as a fluorescent probe and has high selectively effect on Fe(III) ions in ethanol, as well as in water." @default.
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- W3217606906 date "2022-03-01" @default.
- W3217606906 modified "2023-10-01" @default.
- W3217606906 title "A two-dimensional framework with U-shaped Cu4I4 Cluster linked by semi-rigid ligand: Synthesis, crystal structure and Luminescent Properties" @default.
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- W3217606906 doi "https://doi.org/10.1016/j.molstruc.2021.131958" @default.
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