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W330647687 abstract "Electrolytic reduction of uranyl nitrate solutions has been successfully used to prepare pure aqueous and TBP/SST uranium (IV) nitrate solutions for analytical purposes. It has also been used to produce hydrazine-nitrate-stabilized aqueous uranium (IV) nitrate solutions for use as plutonium reductant in a 'Purex' type aqueous reprocessing plant. Unstabilized aqueous and TBP/SST solutions containing more than 99.9% uranium (IV) have been prepared by using an electrolytic cell with platinum electrodes. For plant use, two types of cell have been developed. Both have a platinum anode, but differ in using mercury or platinum as cathode material. Overall and differential current efficiencies of 100% have been obtained at current densities of 250 mA/cm2 for up to 50% uranium (VI) conversion; for 85% conversion the overall and differential current efficiencies are 90% and 65% respectively. (auth)" @default.
W330647687 created "2016-06-24" @default.
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W330647687 date "1966-07-01" @default.
W330647687 modified "2023-09-27" @default.
W330647687 title "STUDY OF URANIUM(IV) NITRATE AS REDUCTANT FOR PLUTONIUM. I. THE PREPARATION OF URANIUM(IV) NITRATE SOLUTIONS. Technical Report No. 118." @default.
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