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- W334595981 abstract "Abstract Nine laboratories collaboratively studied a method for the quantitative GLC determination of lactic and succinic acids in eggs. Four of the laboratories also analyzed samples by the official AOAC method (16.037–16.042). Samples of frozen whole egg, some passable and some decomposed, were analyzed. The organic acids were extracted by the present AOAC procedures, the acids were then esterified with BF2-l-propanol, and the esters were quantitated by GLC. A collaborative report already published on the GLC determination of standard lactic and succinic acids added to egg extracts established that the method gives accurate results over a broad range of acid concentrations. The samples in the present study contained 4–30 mg lactic acid/100 g egg and 0–20 mg succinic acid/100 g egg. Each collaborator analyzed three samples in duplicate and one sample in triplicate. Using the GLC method, the standard deviation was never greater than 0.6 mg for samples containing less than 16 mg lactic acid/100 g egg, while the standard deviation was 0.2 mg for 7 mg or less succinic acid/100 g egg. The results demonstrate that the method gives good precision when it is applied to passable and to decomposed egg and the method is recommended for adoption as official first action." @default.
- W334595981 created "2016-06-24" @default.
- W334595981 creator A5081841191 @default.
- W334595981 date "1970-01-01" @default.
- W334595981 modified "2023-09-26" @default.
- W334595981 title "Collaborative Study on the GLC and AOAC Methods for the Quantitative Determination of Lactic and Succinic Acids in Egg" @default.
- W334595981 doi "https://doi.org/10.1093/jaoac/53.1.28" @default.
- W334595981 hasPublicationYear "1970" @default.
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