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- W337388670 abstract "The optical detection method was used to take the ESR spectra of the (durene)/sup +//(deuteroanthracene)/sup -/ and (triethylamine)/sup +//(deuteroanthracene)/sup -/ radical-ion pairs. Such pairs arise in the irradiation of solutions containing 0.001 M deuteroanthracene (A) and 0.01 M durene (D) or triethylamine (TEA) in squalane (S). In this experiment, the optical detection unit is an attachment to a standard ESR spectrometer consisting of a source of ionizing radiation and photomultiplier activated instead of the ultrahigh-frequency detector of the spectrometer. The system used a BSV-23 x-ray tube with a molybdenum anode as the radiation source. The tube axis was parallel to the magnet axis. The exit window of the tube was 160 mm from the surface of the sample located in a quartz diameter with 11.5 mm diameter in the center of the probe of a Varian E-3 ESR spectrometer. The cell was covered with a cup-like teflon stopper to keep atmospheric oxygen from the sample. The stopper contacted the sample surface. The x-ray radiation hit the sample after passing through a 0.5-mm-thick Teflon layer. The irradiated sample surface was 0.5 cm/sup 2/ in area. A quartz light conductor 9 mm in diameter and 0.5 m in length was attached tomore » the lower edge of the cell. This device was used to conduct light from the sample to an FEU-130 photomultiplier in a Permalloy screen. The signal was transferred from the photomultiplier anode to the inlet of the synchronous detection block of the E-3 ESR spectrometer.« less" @default.
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- W337388670 date "1982-04-01" @default.
- W337388670 modified "2023-09-28" @default.
- W337388670 title "Optical recording of the ESR spectra of short-lived radical-ion pairs by synchronous detection using x-ray irradiation" @default.
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