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- W37481002 abstract "It has been demonstrated that cross-polarization/magic-angle spinning (CP/MAS) nuclear magnetic resonance (NMR) spectroscopy is the most powerful means available to characterize the structure and dynamics of inorganic polymers in the solid state. The most recent development of a variable-temperature (VT) spinner provided an indispensable means to study slow chemical exchange, molecular motion, and phase transitions of inorganic polymers. This chapter reviews the applications of the solid-state multinuclear NMR methods to several inorganic polymers. Solid-state multinuclear NMR experiments have successfully provided very useful information about inorganic-polymer conformations. The structural behaviors of several substituted polysilanes in inorganic polymers were studied in the chapter by means of 29 Si CP/MAS NMR spectroscopy over a wide range of temperatures. The dynamics experiments of these polysilanes were also undertaken through 29 SiT 1 measurements. To consider the relationship between the silicon chemical shift and silicon bond conformation, 29 Si-chemical shifts were calculated by the finite perturbation theory (FPT) CNDO/2 MO method." @default.
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- W37481002 date "1998-01-01" @default.
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- W37481002 title "Inorganic Polymers" @default.
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- W37481002 doi "https://doi.org/10.1016/s0167-6881(98)80025-6" @default.
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