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• W389339375 abstract "Double perovskite related oxide A2ZnTiO6A=Pr, Gd were synthesized by the solid state reaction method at 1523 K. The structure and microstructure of the compounds were studied by X-ray, SAED and FESEM. Rietveld refinement of the powder X-ray analysis shows that the compounds crystallizes in monoclinic space group P21/n (a+b−b−) with unit cell parameter √2ap×√2ap×2ap (a=5.5026(1) Å, b=5.6305(1) Å, c=7.8149(1) Å, β=90.02(1)° for Pr2ZnTiO6 and a=5.3621(1) Å, b=5.6565(2) Å, c=7.6779(2) Å and β=90.264(2)° for Gd2ZnTiO6. Electron diffraction study confirms P21/n symmetry of the oxides. The monoclinic distortion is larger in Gd2ZnTiO6 than Pr2ZnTiO6 which is associated with the tolerance factor and the tilting angle of ZnO6 and TiO6 octahedra (ϕ=13.64° for Pr2ZnTiO6 and 16.51° for Gd2ZnTiO6). The compounds are highly ordered. The charge and size difference between B site cations are the driving force for the ordering of the B′O6 and B″O6 octahedra. Pr2ZnTiO6 shows a dielectric constant of 27 and dielectric loss of 0.003 while Gd2ZnTiO6 has a dielectric constant of 17 and dielectric loss of 0.005 measured at 1 MHz." @default.
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• W389339375 date "2015-09-01" @default.
• W389339375 modified "2023-10-17" @default.
• W389339375 title "Monoclinically distorted perovskites, A2ZnTiO6 (A=Pr, Gd): Rietveld refinement, and dielectric studies" @default.
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• W389339375 doi "https://doi.org/10.1016/j.jssc.2015.05.003" @default.
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