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- W39822021 abstract "The studies of this dissertation are composed of two sections. The first one deals with the analysis of compositional monosaccharides of transgenic corn glycoproteins. The method used in this study involves derivatization of monosaccharides with two fluorophores followed by HPLC/fluorescence detection for quantitative studies, and by HPLC/SSI/MS for identification confirmation of individual monosaccharide. The derivatization process adds a moderate polar moiety to monosaccharides, changing their structures and improving the separation of derivatized monosaccharides on C-18 column, as well as increasing the detection sensitivity dramatically. Moreover, derivatization process also adds a proton receptor to monosaccharide molecules, making them much easier to be ionized by ESI, SSI, APCI, etc. The second section investigates the degradation processes of several pesticides including diazinon, fonofos and aldicarb in various oxidation systems. This oxidation process may result in the formation of oxidation byproducts from the parent pesticides, which could be more toxic than the parent pesticides. Diazoxon and 2-Isopropyl-6-methyl-4-pyrimidinol (IPMP) were detected as the degradation products of diazinon; fonofos oxygen analog was identified to be the degradation product of fonofos, while thiophenol and phenyl disulfide were identified as the alkaline hydrolysis products of fonofos; aldicarb sulfoxide, aldicarb sulfone and N-chloro-aldicarb sulfone were detected as the degradation products of aldicarb. Quantitative studies are also carried out to provide information for kinetics of these oxidation processes." @default.
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- W39822021 date "2007-01-01" @default.
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- W39822021 title "Hyphenated HPLC-MS technique for analysis of compositional monosaccharides of transgenic corn glycoprotein and characterization of degradation products of diazinon, fonofos and aldicarb in various oxidation systems" @default.
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