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- W415782242 abstract "Abstract Conductive polymer based on chitosan has been successfully prepared via solution casting technique with ionic liquid 1-butyl-3-methylimidazolium acetate ([Bmim][OAc]). [Bmim][OAc] plays two important roles in the conduction of chitosan: i) charge carrier and ii) plasticizer in this system. Appearance of new peaks and shifting of several characteristic peaks in the FTIR spectra signify the strong interactions between chitosan and [Bmim][OAc]. XRD diffractograms showed an increase in the amorphous region as the weight percentage (wt.%) of [Bmim][OAc] increases. SEM observations have proven the smoother surface morphology of the plasticized chitosan. The enhancement in the ionic conductivity (σ), is observed as the wt.% of [Bmim][OAc] increases. The highest σ achieved is (2.44 ± 0.41) × 10− 3 S cm− 1 measured at ambient temperature (298 K) and the corresponding activation energy is 0.2961 eV. The temperature dependence of conductivity is Arrhenian in the studied temperature range and achieved σ of (7.60 ± 0.62) × 10− 3 S cm− 1 at 70 °C. The increase in the ionic conductivity is related to the decrease of glass transition temperature (Tg) as proven by the DSC analysis. High electrochemical stability of 3.4 V was achieved of the highest conducting electrolyte by means of linear sweep voltammetry (LSV). Transference number measurement confirms that ions predominate the conduction of electrolyte with 0.75 ion transference number." @default.
- W415782242 created "2016-06-24" @default.
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- W415782242 date "2015-10-01" @default.
- W415782242 modified "2023-10-12" @default.
- W415782242 title "Bifunctional ionic liquid in conductive biopolymer based on chitosan for electrochemical devices application" @default.
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- W415782242 doi "https://doi.org/10.1016/j.ssi.2015.05.008" @default.
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