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- W4200051546 abstract "A Ru(II)-catalyzed regioselective direct ortho-amidation of 2-aryl benzo[d]thiazoles employing acyl azides as a nitrogen source has been accomplished. This approach utilizes the efficiency of benzothiazole as a directing group and the role of acyl azide as an effective amidating agent toward C-N bond formation, thereby evading the general Curtius rearrangement. The protocol highlights significant functional group tolerance, single-step, and external oxidant-free conditions, with the release of only innocuous molecular nitrogen as the byproduct. The reaction mechanism and the intermediates associated with this selective Ru-catalyzed reaction have been investigated using ESI-MS. The protocol also aided in the construction of ortho-amidated β-carbolines, unveiling another class of fluorescent molecules." @default.
- W4200051546 created "2021-12-31" @default.
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- W4200051546 date "2021-12-27" @default.
- W4200051546 modified "2023-10-11" @default.
- W4200051546 title "Ru(II)-Catalyzed Regioselective C–N Bond Formation on Benzothiazoles Employing Acyl Azide as an Amidating Agent" @default.
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- W4200051546 doi "https://doi.org/10.1021/acsomega.1c05910" @default.
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