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- W4200114966 abstract "We demonstrate a method for the synthesis of a water-soluble multimetallic peptidic array containing a predetermined sequence of metal centers such as Ru(II), Pt(II), and Rh(III). The compound, named as a water-soluble metal-organic complex array (WSMOCA), is obtained through 1) the conventional solution-chemistry-based preparation of the corresponding metal complex monomers having a 9-fluorenylmethyloxycarbonyl (Fmoc)-protected amino acid moiety and 2) their sequential coupling together with other water-soluble organic building units on the surface-functionalized polymeric resin by following the procedures originally developed for the solid-phase synthesis of polypeptides, with proper modifications. Traces of reactions determined by mass spectrometric analysis at the representative coupling steps in stage 2 confirm the selective construction of a predetermined sequence of metal centers along with the peptide backbone. The WSMOCA cleaved from the resin at the end of stage 2 has a certain level of solubility in aqueous media dependent on the pH value and/or salt content, which is useful for the purification of the compound." @default.
- W4200114966 created "2021-12-31" @default.
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- W4200114966 date "2016-10-08" @default.
- W4200114966 modified "2023-09-26" @default.
- W4200114966 title "Synthesis of a Water-soluble Metal–Organic Complex Array" @default.
- W4200114966 doi "https://doi.org/10.3791/54513-v" @default.
- W4200114966 hasPublicationYear "2016" @default.
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