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• W4200215280 abstract "Amorphous, polymeric molybdenum sulfide has attracted significant attention as a non-platinum group electrocatalyst for the hydrogen evolution reaction (HER). To elucidate the influence of oxygen incorporation on molybdenum sulfide catalysts, MoOxSy electrocatalysts were synthesized via a potentiostatic electrodeposition method. The presence of oxygen and the associated molybdenum oxidation state were modified by postsynthesis treatments of air exposure, annealing in an inert atmosphere, and annealing in a sulfur flux. The as deposited sample exhibited the best performance, requiring only 171 mV to reach a cathodic current density of 10 mA/cm2. While the modified films exhibited worse HER performance compared to the as deposited sample, by utilizing extensive X-ray photoelectron spectroscopy studies, we highlighted the importance of the Mo5+ oxidation state while identifying a previously unreported state within MoOxSy catalysts between Mo4+ and Mo5+." @default.
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• W4200215280 date "2021-12-13" @default.
• W4200215280 modified "2023-09-30" @default.
• W4200215280 title "Influence of Oxygen Dopants on the HER Catalytic Activity of Electrodeposited MoO_<i>x</i>S_<i>y</i> Electrocatalysts" @default.
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• W4200215280 doi "https://doi.org/10.1021/acsaem.1c02234" @default.
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