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- W4200263102 abstract "A Bi-catalyzed synthesis of sulfonyl fluorides from the corresponding (hetero)aryl boronic acids is presented. We demonstrate that the organobismuth(III) catalysts bearing a bis-aryl sulfone ligand backbone revolve through different canonical organometallic steps within the catalytic cycle without modifying the oxidation state. All steps have been validated, including the catalytic insertion of SO2 into Bi-C bonds, leading to a structurally unique O-bound bismuth sulfinate complex. The catalytic protocol affords excellent yields for a wide range of aryl and heteroaryl boronic acids, displaying a wide functional group tolerance." @default.
- W4200263102 created "2021-12-31" @default.
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- W4200263102 date "2021-12-16" @default.
- W4200263102 modified "2023-10-18" @default.
- W4200263102 title "Redox-Neutral Organometallic Elementary Steps at Bismuth: Catalytic Synthesis of Aryl Sulfonyl Fluorides" @default.
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- W4200263102 doi "https://doi.org/10.1021/jacs.1c11463" @default.
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