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• W4200403604 abstract "A convenient, efficient, and general procedure for the synthesis of diaryl diselenides has been developed by the reaction of aryl diazonium tetrafluoroborates and Potassium Selenocyanate on the surface of alumina under ball-milling in absence of any solvent, transition metal catalyst and base in room temperature. A wide range of functionalized diaryl diselenides are obtained in high purity and high yield by this procedure.Synthesis of diaryl diselenides was restricted into only few Cu-catalyzed C-Se Cross coupling protocol where use of ligands, high reaction temp, long reaction time were required.To achieve a sustainable protocol for the synthesis of diaryl diselenides Method: Reaction of aryl diazonium fluoroborate with KSeCN was successfully performed under ball milling in absence of any ransition metal catalyst, ligands, base and external heating to get diaryl diselenides.A library of diaryl diselenides were obtained in good yields with different functional groups.First transition metal free protocol for the synthesis of diaryl diselenides has been developed successfully." @default.
• W4200403604 created "2021-12-31" @default.
• W4200403604 creator A5058444513 @default.
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• W4200403604 date "2022-06-01" @default.
• W4200403604 modified "2023-09-27" @default.
• W4200403604 title "Transition Metal Catalyst, Solvent, Base Free Synthesis of Diaryl Diselenides under Mechanical Ball Milling" @default.
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• W4200403604 doi "https://doi.org/10.2174/1570179419666211224144932" @default.
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