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- W4200538047 abstract "Two amorphous BCN–SiC composites, sample BSC (BN + SiC + C) and sample BCSA (B2O3+C + Si + AlN) were prepared from different raw materials via spark plasma sintering (SPS) for 5 min at 1670 °C under a pressure of 30 MPa. Sample BCSA was found to generally outperform sample BSC, and its relative density (99.13% vs. 97.28%), flexural strength (453.1 MPa vs. 334.5 MPa), Vickers’ hardness (19.15 GPa vs. 16.53 GPa), and fracture toughness (5.21 MPa m1/2 vs. 3.76 MPa m1/2). The solid-phase reactions in the binary (sample BSC) and quaternary (sample BCSA) systems were elucidated from X-ray diffraction (XRD), energy dispersive spectroscopy (EDS), and thermodynamic calculations. The microstructure of the composites, which were synthesized from two different materials, was also characterized. The grain size and aspect ratio of the lamellar amorphous BCN grains played an important role in improving the mechanical properties of the composites. High-resolution transmission electron microscopy (HRTEM) and selected area electron diffraction (SAED) were used to clarify the microstructure of the amorphous phase of BCN and its interfacial area. Based on these results, element diffusion was discussed. The mechanism for the microstructural evolution and phase transformation of the composite were also discussed." @default.
- W4200538047 created "2021-12-31" @default.
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- W4200538047 date "2022-03-01" @default.
- W4200538047 modified "2023-10-16" @default.
- W4200538047 title "Microstructure evolution and phase transformation of amorphous BCN–SiC composites prepared by two synthetic routes" @default.
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- W4200538047 doi "https://doi.org/10.1016/j.ceramint.2021.11.323" @default.
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