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- W4200547711 abstract "Abstract The crystal structures of the M(SbF 6 ) 2 salts (M=Cu, Pd) are isotypic (Type I) . They crystallize in the triclinic space group , Z =1 at 150 K. M 2+ cations lying in the same plane are connected via SbF 6 units forming slabs. There are only van der Waals contacts of fluorine atoms between the adjacent slabs. Salts of M(SbF 6 ) 2 (M=Fe, Co, Zn) crystallize differently (Type II ; space group , Z =2 at 150 K). Their crystal structures are composed of M 2+ cations interconnected by [SbF 6 ] − anions – thus forming a three‐dimensional framework. The crystal structure of Fe(SbF 6 ) 2 , determined at 240 K, is currently the only representative of the Type III . The main feature of this type is also a three‐dimensional framework consisting of M 2+ cations and [SbF 6 ] − anions. However, the mode of their association differs from that observed in Type II . The crystal structures of CuFSbF 6 (orthorhombic space group Imma , Z=4 at 150 K) and AgFSbF 6 (orthorhombic space group Pnma , Z= 4 at 150 K) are not isotypic. The crystal structures of the by‐products H 3 ONi(SbF 6 ) 3 (orthorhombic space group Pnma , Z=4 at 150 K) and (O 2 ) 2 Ag 6 CuF 5 (SbF 6 ) 11 ⋅ 2HF (triclinic space group , Z =1 at 150 K) were determined. In the latter, HF is directly attached to an Ag(II) via a fluorine atom." @default.
- W4200547711 created "2021-12-31" @default.
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- W4200547711 date "2022-01-27" @default.
- W4200547711 modified "2023-10-14" @default.
- W4200547711 title "Crystal Structures of Hexafluoridoantimonate(V) Salts of d‐block Metals in Oxidation State +2" @default.
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- W4200547711 doi "https://doi.org/10.1002/ejic.202101076" @default.
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