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- W4200564382 abstract "Abstract Herein we report the synthesis of the new statin derivative MC609 in 80 % overall yield by sequential transformation of simvastatin including dehydration, and Michael addition of N ‐benzyl hydroxylamine followed by cyclization. The preparation of nitronestatins MC649 and MC645 is also described from (2 S ,4 R )‐4‐(( tert ‐butyldimethylsilyl)oxy)‐6‐oxotetrahydro‐2 H ‐pyran‐2‐carbaldehyde by reaction with N ‐benzyl hydroxylamine, and N ‐hydroxylamine followed by reduction with sodium cyanoborohydride and coupling with commercially available 2‐chloro‐6‐methylquinoline‐3‐carbaldehyde, in 77 % and 24 % overall yield, respectively." @default.
- W4200564382 created "2021-12-31" @default.
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- W4200564382 date "2021-12-16" @default.
- W4200564382 modified "2023-10-05" @default.
- W4200564382 title "Synthesis of New Statin Derivatives" @default.
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- W4200564382 doi "https://doi.org/10.1002/slct.202103544" @default.
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