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- W4200590015 abstract "An efficient I2/K2S2O8-promoted ring expansion of benzo[d]thiazole and 3-oxo-3-arylpropanenitrile has been developed. A variety of benzo[d]thiazole derivatives underwent the ring-opening cyclization smoothly to afford the diverse 3-aryl-4H-benzo[b][1,4]thiazine-2-carbonitriles in moderate to excellent yields. This protocol features metal-free reaction conditions, stable and available starting materials, and good group tolerance. The synthetic utility of this protocol was also demonstrated through gram-scale reaction and product derivatization. Mechanism studies indicate that the reaction may undergo a free radical process." @default.
- W4200590015 created "2021-12-31" @default.
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- W4200590015 date "2022-01-01" @default.
- W4200590015 modified "2023-09-26" @default.
- W4200590015 title "I2/K2S2O8-Promoted ring-opening cyclizations of benzothiazoles and 3-oxo-3-arylpropanenitriles" @default.
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- W4200590015 doi "https://doi.org/10.1016/j.mcat.2021.112051" @default.
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