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• W4200607931 endingPage "123504" @default.
• W4200607931 startingPage "123504" @default.
• W4200607931 abstract "β -PbO 2 is an important high oxygen overpotential anode coating material. Further study on nanoscale β -PbO 2 with higher performance and lower cost is a critical issue in order to develop the electrochemical ozone generator. Herein, an improved β -PbO 2 nanoparticles synthesizing strategy based on the traditional Pb(OAc) 4 hydrolysis method is proposed in this work, which is more scalable for industrial-scale production compared with existed nano β -PbO 2 synthesizing methods. The possible mechanism of synthesizing β -PbO 2 nanoparticles via Pb(OAc) 4 hydrolysis was discussed for the first time. Based on the proposed mechanism, the size and morphology of the β -PbO 2 nanoparticles were effectively controlled, and alternative raw material that can significantly reduce costs was developed. SEM, TEM, XRD, and XPS results indicate that pure phase β -PbO 2 nanoparticles range from 10–30 nm were obtained. In addition, the use of alternative raw materials reduces the cost by 90%–95% compared to the traditional Pb(OAc) 4 hydrolysis method. The β -PbO 2 nanoparticles showed good ozone generation performances. The energy consumption per unit ozone of the β -PbO 2 nanoparticles is reduced by 51.9% at the optimized operation condition than the reference PbO 2 particles used for comparison." @default.
• W4200607931 created "2021-12-31" @default.
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• W4200607931 date "2021-12-01" @default.
• W4200607931 modified "2023-10-16" @default.
• W4200607931 title "Facile Synthesis of β-PbO₂ Nanoparticles Range from 10–30 nm and their Application for Ozone Generation" @default.
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• W4200607931 doi "https://doi.org/10.1149/1945-7111/ac40c6" @default.
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