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- W4206064099 abstract "Glycerol acetalization with citral was studied using a heteropolyacid (tungstophosphoric acid) supported on KIT-6, as a catalyst, at 100 °C. Different catalysts were synthesized. Catalysts were characterized by scanning electron microscopy (SEM), inductively coupled plasma (ICP), X-ray diffraction (XRD), attenuated total refletion-Fourier transform infrared spectroscopy (ATR-FTIR), and potentiometric titrations. At a fixed time, the glycerol conversion increased with the H3PW12O40 (PW) on KIT-6. PW4-KIT-6 material had a higher conversion than other catalysts. The optimization of glycerol’s acetalization with citral was studied under the PW4-KIT-6 catalyst. After 5 h, it was found that, at T = 100 °C, with m = 0.3 g of solid, molar glycerol:citral = 1:2.25, the conversion of glycerol was 89%. Moreover, the PW4-KTI-6 catalyst showed good catalytic stability." @default.
- W4206064099 created "2022-01-25" @default.
- W4206064099 creator A5052226267 @default.
- W4206064099 date "2022-01-12" @default.
- W4206064099 modified "2023-09-27" @default.
- W4206064099 title "Acetalization of Glycerol with Citral over Heteropolyacids Immobilized on KIT-6" @default.
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- W4206064099 doi "https://doi.org/10.3390/catal12010081" @default.
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