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• W4206199082 abstract "An elegant and catalytic procedure for the one-step cyanomethylenation of C(sp3)-H bonds adjacent to benzazoles and ketones is described herein using DMF as a C-1 unit and TMSCN as the cyanide source. The copper-mediated reaction between DMF and TMSCN gives a cyanomethylene radical intermediate that reacts with 2-alkylbenzazoles or alkylketones to furnish desired cyanomethylenated compounds under palladium catalysis. Subsequent interconversion of cyanomethylenated products makes the protocol synthetically attractive." @default.
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• W4206199082 date "2022-01-10" @default.
• W4206199082 modified "2023-10-15" @default.
• W4206199082 title "Catalytic Direct Cyanomethylenation of C(sp³)–H Bonds via a One-Step Double C–C Bond Formation" @default.
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• W4206199082 doi "https://doi.org/10.1021/acs.joc.1c02297" @default.
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