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• W4207076688 abstract "The rising interest in advances of sustainable and greener synthetic approaches has encouraged chemists to investigate novel methods to stimulate organic compounds. The benzyl alcohol and its derivatives are industrially significant chemicals owing to their huge applications in petrochemical industries. In this context a green and sustainable approach for synthesis of Chloro substituted benzyl alcohols has been established. In present research paper cyclic voltammetry study followed by constant current electrolysis and characterization of synthesized 2-Chlorobenzyl alcohol, 3-Chlorobenzyl alcohol, 4-Chlorobenzyl alcohol and 2,4-Dichlorobenzyl alcohol has been reported. Cyclic voltammetry measurements have been employed to setup optimum conditions for electrolysis and to find out electrochemical nature of various Chloro substituted benzaldehydes. Then these results have been judiciary used to carry out electrochemical reduction of various Chloro substituted benzaldehydes using constant current electrolysis. Influence of scan rate and pH on reduction peaks has also been investigated referring irreversible electron transfer phenomenon in basic medium. The kinetic parameters for reduction reactions have been estimated showing the process under the influence of diffusion control. The characterization of electrochemically synthesized 2-Chlorobenzyl alcohol, 3-Chlorobenzyl alcohol, 4-Chlorobenzyl alcohol and 2,4-Dichlorobenzyl alcohol has been done by using spectroscopic techniques such as IR, 1 HNMR and Mass spectral analysis. This has a scientific achievement in terms of the obtained products (2-Chlorobenzyl alcohol, 3-Chlorobenzyl alcohol, 4-Chlorobenzyl alcohol and 2,4-Dichlorobenzyl alcohol) and their derivatives which are industrially and pharmaceutically significant chemicals owing to their huge applications in petrochemical industries and medical sectors. Throat lozenges containing dichlorobenzyl alcohol (DCBA) are used for treatment of respiratory tract infections. Graphical representation for Electro organic synthesis. • 2-Chlorobenzyl alcohol, 3-Chlorobenzyl alcohol, 4-Chlorobenzyl alcohol and 2,4-Dichlorobenzyl alcohol has been synthesized by electrochemical reduction of corresponding Chloro substituted benzaldehydes. • Cyclic voltammetry study followed by constant current electrolysis has been carried out. • Synthesized Chloro substituted benzyl alcohols have been characterized using spectroscopic techniques." @default.
• W4207076688 created "2022-01-26" @default.
• W4207076688 creator A5035026051 @default.
• W4207076688 date "2022-01-01" @default.
• W4207076688 modified "2023-09-26" @default.
• W4207076688 title "Electro organic synthesis as green and sustainable approach for synthesis of chloro substituted benzyl alcohols" @default.
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• W4207076688 doi "https://doi.org/10.1016/j.jics.2022.100365" @default.
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