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- W4207089350 abstract "Abstract Well‐defined glyco‐polyorganosiloxanes were synthesized by the Cu( I )‐catalyzed Huisgen 1,3‐dipolar cycloaddition reaction (often simply referred to as “click” chemistry). N ‐propargylglycosylamines 2 and 4 were first synthesized from cellobiose ( 1 ) and xylogluco‐oligosaccharide XGOs 3 without protecting groups. The azide function was introduced into polydimethylsiloxanes [PDMS: 5 (MD′M) and 7 (M′DM′)] by azidolysis of the counterpart epoxy silicon with NaN 3 to afford the mono‐azido 6 and di‐azido 8 derivatives, respectively. The coupling reaction took place in a hydro‐alcoholic medium in the presence of CuSO 4 /sodium ascorbate as catalyst. Only one compound, MD′M‐“click”‐XGO 12 showed good solubility in water with interesting surfactant properties. magnified image" @default.
- W4207089350 created "2022-01-26" @default.
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- W4207089350 date "2008-06-13" @default.
- W4207089350 modified "2023-10-17" @default.
- W4207089350 title "Syntheses of Well-Defined Glyco-Polyorganosiloxanes by “Click” Chemistry and their Surfactant Properties" @default.
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- W4207089350 doi "https://doi.org/10.1002/macp.200700629" @default.
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