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- W4210456750 abstract "This study aims at preparing novel composite materials for the consolidation of damaged stone in built heritage from tetraethoxysilane(TEOS)based sols with nano-sized hydroxyapatite (HAp) with high crystallinity and high aspect ratio. Synthesis of nanostructures of hydroxyapatite (HAp) was carried out using hydrothermal precipitation methods at different reaction temperatures and periods. Rod-like HAp nanostructures with a diameter around 5–20 nm and length up to 125 nm were obtained. The samples of nano-HAp were characterised using powder X-ray diffraction (XRD), Transmission Electron Microscopy (TEM) and μ-Raman spectroscopy. The derived nanostructures were used to modify TEOS-based formulations after tuning their colloidal stability period to the needs of their application as stone consolidants. The chemical structure (μ-Raman), viscosity, macroscopic and microscopic morphologies – Scanning Electron Microscopy (SEM) and EDS – and Shore Hardness of the composite materials were studied. The potential of the composite materials containing nano-HAp-rods as stone consolidants revealed to be superior to the potential of reference materials." @default.
- W4210456750 created "2022-02-08" @default.
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- W4210456750 date "2022-05-01" @default.
- W4210456750 modified "2023-10-14" @default.
- W4210456750 title "Synthesis and application of hydroxyapatite nanorods for improving properties of stone consolidants" @default.
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- W4210456750 doi "https://doi.org/10.1016/j.ceramint.2022.02.004" @default.
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