Matches in SemOpenAlex for { <https://semopenalex.org/work/W4212915678> ?p ?o ?g. }
- W4212915678 endingPage "5356" @default.
- W4212915678 startingPage "5349" @default.
- W4212915678 abstract "Two dimensional (2D) 1H-13C heteronuclear single-quantum correlation (HSQC) spectroscopy has recently been proposed for quantitative determination of typical linear low density polyethylene (LLDPE) with high accuracy. It requires highly precise measurement to achieve further reliable quantification. In this context, this paper aims at determining conditions that allow the achievement of high precision. On the basis of the optimized parameters, two time-saving strategies, nonuniform sampling (NUS) and band-selective HSQC are evaluated on model polyolefins in terms of repeatability. Precision better than 0.3% and 5% for ethylene content (E mol%) and 1-hexene content (H mol%) of the model poly(ethylene-co-1-hexene)s are obtained with 50% NUS or band-selective HSQC. Moreover, dramatic precision enhancements can be achieved with the combination of band-selective HSQC and 50% NUS, in which repeatabilities better than 0.15% and 2.5% for E mol% and H mol% are observed. The experiment times are reduced to about 0.5 h. These methods open important perspectives for rapid, precise and accurate quantitative analysis of complex polymers." @default.
- W4212915678 created "2022-02-24" @default.
- W4212915678 creator A5028249096 @default.
- W4212915678 creator A5047307531 @default.
- W4212915678 creator A5073575637 @default.
- W4212915678 date "2022-01-01" @default.
- W4212915678 modified "2023-09-30" @default.
- W4212915678 title "Rapid quantitative 1H–13C two-dimensional NMR with high precision" @default.
- W4212915678 cites W1525440618 @default.
- W4212915678 cites W1542229172 @default.
- W4212915678 cites W1963654759 @default.
- W4212915678 cites W1967144552 @default.
- W4212915678 cites W1979243955 @default.
- W4212915678 cites W1980218660 @default.
- W4212915678 cites W1984990753 @default.
- W4212915678 cites W1985105730 @default.
- W4212915678 cites W1988509628 @default.
- W4212915678 cites W1991763410 @default.
- W4212915678 cites W1993877487 @default.
- W4212915678 cites W1996222877 @default.
- W4212915678 cites W1997028373 @default.
- W4212915678 cites W1998907791 @default.
- W4212915678 cites W2019049656 @default.
- W4212915678 cites W2022768923 @default.
- W4212915678 cites W2024755768 @default.
- W4212915678 cites W2026040227 @default.
- W4212915678 cites W2031267461 @default.
- W4212915678 cites W2036583236 @default.
- W4212915678 cites W2046143330 @default.
- W4212915678 cites W2046152748 @default.
- W4212915678 cites W2049454380 @default.
- W4212915678 cites W2055254541 @default.
- W4212915678 cites W2055984947 @default.
- W4212915678 cites W2058241083 @default.
- W4212915678 cites W2063028841 @default.
- W4212915678 cites W2063214203 @default.
- W4212915678 cites W2073306116 @default.
- W4212915678 cites W2079171083 @default.
- W4212915678 cites W2082461561 @default.
- W4212915678 cites W2085372822 @default.
- W4212915678 cites W2090998045 @default.
- W4212915678 cites W2110199583 @default.
- W4212915678 cites W2137876183 @default.
- W4212915678 cites W2161469143 @default.
- W4212915678 cites W2164906387 @default.
- W4212915678 cites W2315744637 @default.
- W4212915678 cites W2320074788 @default.
- W4212915678 cites W2324166983 @default.
- W4212915678 cites W2332432279 @default.
- W4212915678 cites W2332791358 @default.
- W4212915678 cites W2334707000 @default.
- W4212915678 cites W2341460985 @default.
- W4212915678 cites W2346786297 @default.
- W4212915678 cites W2487803538 @default.
- W4212915678 cites W2572088127 @default.
- W4212915678 cites W2582851884 @default.
- W4212915678 cites W2623022748 @default.
- W4212915678 cites W2915363601 @default.
- W4212915678 cites W2956088129 @default.
- W4212915678 cites W3182481313 @default.
- W4212915678 doi "https://doi.org/10.1039/d1ra08423b" @default.
- W4212915678 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/35425561" @default.
- W4212915678 hasPublicationYear "2022" @default.
- W4212915678 type Work @default.
- W4212915678 citedByCount "1" @default.
- W4212915678 countsByYear W42129156782023 @default.
- W4212915678 crossrefType "journal-article" @default.
- W4212915678 hasAuthorship W4212915678A5028249096 @default.
- W4212915678 hasAuthorship W4212915678A5047307531 @default.
- W4212915678 hasAuthorship W4212915678A5073575637 @default.
- W4212915678 hasBestOaLocation W42129156781 @default.
- W4212915678 hasConcept C113196181 @default.
- W4212915678 hasConcept C151730666 @default.
- W4212915678 hasConcept C154020017 @default.
- W4212915678 hasConcept C161790260 @default.
- W4212915678 hasConcept C178790620 @default.
- W4212915678 hasConcept C185592680 @default.
- W4212915678 hasConcept C186060115 @default.
- W4212915678 hasConcept C192562407 @default.
- W4212915678 hasConcept C193125475 @default.
- W4212915678 hasConcept C19549132 @default.
- W4212915678 hasConcept C2778597550 @default.
- W4212915678 hasConcept C2779343474 @default.
- W4212915678 hasConcept C43617362 @default.
- W4212915678 hasConcept C66974803 @default.
- W4212915678 hasConcept C71240020 @default.
- W4212915678 hasConcept C86803240 @default.
- W4212915678 hasConcept C92381491 @default.
- W4212915678 hasConceptScore W4212915678C113196181 @default.
- W4212915678 hasConceptScore W4212915678C151730666 @default.
- W4212915678 hasConceptScore W4212915678C154020017 @default.
- W4212915678 hasConceptScore W4212915678C161790260 @default.
- W4212915678 hasConceptScore W4212915678C178790620 @default.
- W4212915678 hasConceptScore W4212915678C185592680 @default.
- W4212915678 hasConceptScore W4212915678C186060115 @default.
- W4212915678 hasConceptScore W4212915678C192562407 @default.
- W4212915678 hasConceptScore W4212915678C193125475 @default.
- W4212915678 hasConceptScore W4212915678C19549132 @default.