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• W4213014658 abstract "Probing short-lived reaction species is challenging owing to the need for both high signal-to-noise ratio, which can require long measurement time, and fast time resolution. Here, a novel in situ sample environment is presented that decouples time resolution from measurement time by distributing reaction time over space for the reaction under flow. In the mixing-flow reactor, precursor solutions are mixed at a specific position along the flow path, where the reaction is initiated. As the reaction mixture flows within a reaction capillary, the reaction time increases with distance from the mixing point. A measurement can be taken at a specific distance from the mixing point for as long as is needed to accumulate good statistics without compromising the time resolution of the measurement. Applications of the mixing-flow reactor for pair distribution function measurements of the initial nuclei formed during the hydrolysis of Al 3+ at high pH are shown." @default.
• W4213014658 created "2022-02-24" @default.
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• W4213014658 date "2022-02-16" @default.
• W4213014658 modified "2023-10-16" @default.
• W4213014658 title "A mixing-flow reactor for time-resolved reaction measurements distributed in space" @default.
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• W4213014658 doi "https://doi.org/10.1107/s1600576722000620" @default.
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