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- W4220792457 abstract "In the present research, the influence of TiN addition on the ZrB2–SiC composite was studied. Hereof, TiN-doped ZrB2–SiC composite was manufactured via the route of reactive spark plasma sintering under an applied load of 40 MPa at the peak temperature of 1850 °C for 360 s. Mechanical properties, microstructure evaluation, and sinterability were investigated and compared to the non-doped ZrB2–SiC. X-ray diffraction analysis, thermodynamic appraisal, energy dispersive spectroscopy, and scanning electron microscopy divulged the formation of in-situ h-BN, ZrO2, and ZrN as well as the (Zr,Ti)B2 solid solution in TiN-doped ZrB2–SiC. Comparing the relative density of 95% for the TiN-free sample with the relative density of 94.1% for the sample containing TiN, the addition of TiN increased porosity content owing to the formation of in-situ BN with layered structure. Flexural strength decreased from 460.2 MPa for TiN-free ZrB2–SiC to 435.9 MPa for TiN-doped ZrB2–SiC, due to matrix grain growth and relative density drop. In contrast, indentation fracture toughness and Vickers hardness increased to 6.1 MPa.m1/2 and 29.1 GPa, respectively, as the result of TiN addition." @default.
- W4220792457 created "2022-04-03" @default.
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- W4220792457 date "2022-07-01" @default.
- W4220792457 modified "2023-10-02" @default.
- W4220792457 title "On the reactive spark plasma sinterability of ZrB2–SiC–TiN composite" @default.
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- W4220792457 doi "https://doi.org/10.1016/j.jallcom.2022.164611" @default.
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