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- W4220908511 abstract "Abstract A facile synthesis of low band gap water soluble dyad materials comprising of fullerenol and poly thiophene carboxylic acids is demonstrated. Fullerene‐conjugated polyelectrolytes dyad materials were prepared using polythiophene‐3‐acetic acid (PT3AA) and polythiophene‐3‐malonic acid (PT3MA) as donors and fullerenol as acceptor in microwave synthesizer at 70°C. The reaction has several advantages over conventional reflux methods; easy to handle, fast reaction and good quality products. Fullerene core star‐like dyad structures having single‐ or di‐carboxylic acid group in each thiophene ring were synthesized. Thermal methods (TGA & DSC) estimated about six to seven exohedrally attached polymer units to fullerene core. The electrochemical band gaps of ~1.17 and 1.21 eV were recorded for fullerenol poly thiophene 3‐acetic acid (FPT3AA) and fullerenol polythiophene‐3‐malonic acid (FPT3MA) dyads, respectively. The UV–vis analyses record a red shifting of absorbance maxima for mono carboxylic acid (408 nm FPT3AA vs. 263 nm PT3AA) and blue shifting in di‐carboxylic acid (263 nm FPT3MA vs. 396 nm PT3MA). The strong quenching and substantial red shifting of emission peaks of dyad materials compared to both fullerenol and polymers demonstrate charge transfer exciplex formation in excited state." @default.
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- W4220908511 date "2022-03-07" @default.
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- W4220908511 title "Microwave assisted synthesis of low band gap water soluble dyad materials using polythiophene carboxylic acids as donor and fullerenol as acceptor" @default.
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- W4220908511 doi "https://doi.org/10.1002/app.52305" @default.
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