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- W4220909811 abstract "Abstract A series of new strontium complexes, [Sr(tmtad)(btsa)] 2 ( 1 ), [Sr(ptmtad)(btsa)] 2 ( 2 ), [Sr(etmtad)(btsa)] 2 ( 3 ), [Sr(tmtad)(tmhd)] 2 ( 4 ), [Sr(ptmtad)(tmhd)] 2 ( 5 ), and [Sr(etmtad)(tmhd)] 2 ( 6 ), were successfully synthesized by substitution reactions between btsa, aminoalkoxide ligands, and tmhdH (btsa=bis(trimethylsilyl) amide, tmtadH=2,5,9,12‐tetramethyl‐2,5,9,12‐tetraazatridecan‐7‐ol, ptmtadH=2,5,7,9,12‐pentamethyl‐2,5,9,12‐tetraazatridecan‐7‐ol, etmtadH=7‐ethyl‐2,5,9,12‐tetramethyl‐2,5,9,12‐tetraazatridecan‐7‐ol, tmhdH=2,2,6,6‐tetramethyl‐3,5‐heptanedione). Thermogravimetric analysis (TGA) of the new strontium compounds showed low residual masses (4‐11 %) where complex 4 displayed the highest volatility and thermal stability. Single crystal X‐ray study of complexes 1 , 3 , and 6 revealed that the respective complexes crystalize in a triclinic space group as a dimer with a hexa‐ or hepta‐coordination. Furthermore, dimethylamino nitrogen atoms of aminoalkoxide ligands are freely pendent without coordinating to the central strontium metal due to their steric hindrance on the coordination sphere. Compounds 1–6 were characterized by 1 H‐ and 13 C‐nuclear magnetic resonance (NMR) spectroscopy, Fourier‐transform infrared (FT‐IR) spectroscopy, elemental analysis (EA), and thermogravimetric analysis." @default.
- W4220909811 created "2022-04-03" @default.
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- W4220909811 date "2022-03-23" @default.
- W4220909811 modified "2023-09-26" @default.
- W4220909811 title "Synthesis and Characterization of New Strontium Complexes with Multidentate Ligands" @default.
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- W4220909811 doi "https://doi.org/10.1002/slct.202104606" @default.
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