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• W4221097265 endingPage "7892" @default.
• W4221097265 startingPage "7882" @default.
• W4221097265 abstract "Triphenylpnictogens were oxidized to access diphenylpnictioginic acids Ph2XOOH (X = P, As, Sb, Bi). It was shown that oxidation with chloramine-T does not lead to the cleavage of a C-pnictogen bond. The preliminary reductive cleavage with sodium in liquid ammonia followed by the oxidation with hydrogen peroxide was successfully utilised for the synthesis of diphenylphosphinic and diphenylarsinic acids. It was shown that in solid state (by means of XRD), all diphenylpnictoginic acids form polymeric chains. Diphenylbismuthinic and diphenylantimonic acids form polymeric covalent adducts, while diphenylphosphinic and diphenylarsinic chains are associated through hydrogen bonding. Unlike diphenylphosphinic acid, diphenilarsinic acid forms two polymorphs of hydrogen-bonded infinite chains. In solution in a polar aprotic solvent diphenylarsinic acid, similarly to dimethylarsinic, forms hydrogen-bonded cyclic dimers together with a small amount of cyclic trimers." @default.
• W4221097265 created "2022-04-03" @default.
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• W4221097265 date "2022-01-01" @default.
• W4221097265 modified "2023-09-22" @default.
• W4221097265 title "Self-association of diphenylpnictoginic acids in solution and solid state: covalent <i>vs.</i> hydrogen bonding" @default.
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• W4221097265 doi "https://doi.org/10.1039/d2cp00286h" @default.
• W4221097265 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/35302575" @default.
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