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- W4224074805 abstract "Hinckdentine A, a marine-sponge-derived tribrominated indole alkaloid bearing a unique indolo[1,2-c]quinazoline skeleton, was completed in 12 steps featuring the construction of the Nα-quaternary carbon center by asymmetric azo-ene cyclization. A novel organocatalyst was developed to promote high-yielding tribromination, which represents a challenging process encountered in previous syntheses. Density functional theory calculations scrutinized viable substrates and deciphered the origin of the enhancement of C8 electrophilic bromination with a bifunctional organocatalyst. Moreover, the application of organocatalyst-enabled bromination on various substrates was demonstrated to highlight future late functionalizations of biologically intriguing targets." @default.
- W4224074805 created "2022-04-19" @default.
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- W4224074805 date "2022-04-15" @default.
- W4224074805 modified "2023-09-29" @default.
- W4224074805 title "Total Synthesis of (+)-Hinckdentine A: Harnessing Noncovalent Interactions for Organocatalytic Bromination" @default.
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- W4224074805 doi "https://doi.org/10.1021/jacsau.2c00048" @default.
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