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- W4224289477 abstract "In this study, two compounds of triethylene glycol bistosylate (C20H26O8S2, I) and 1,8-bis(4-nitrophenoxy)-3,6-dioxaoctane (C18H20N2O8, II) were synthesized. Their structures were characterized by 1H NMR, 13C NMR, FT-IR, melting-point and elemental analysis, as well as X-ray single-crystal diffraction. The analyses of X-ray single crystal diffraction showed that the monomer of compound I was in sigmoid conformation due to the intramolecular C-H···π interaction, furthermore, a 3D network structure was constructed by five C-H···O hydrogen bonds. Unlike the compound I, the compound II was linked by two C-H···O hydrogen bonds through nitro and aromatic rings to form a 2D network structure. Host-guest chemistry of compounds II and β-cyclodextrin was also investigated by 1H NMR, FT-IR and UV-Vis spectra. The binding ratio of the compound II and β-cyclodextrin was 1:2 and the association constant Ka was 5.31 × 104 L2·mol−2 obtained by UV-Vis spectra." @default.
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- W4224289477 date "2022-04-19" @default.
- W4224289477 modified "2023-10-16" @default.
- W4224289477 title "Synthesis, characterization and crystal structure of two triethylene glycol derivatives" @default.
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- W4224289477 doi "https://doi.org/10.1080/15421406.2022.2027713" @default.
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