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• W4224303429 abstract "• D-limonene and its oxidation products residues were determined in vegetables and soils by using QuEChERS and GC–MS method. • D-limonene and its oxidation products were not persistent in soil. • Degradation of d -limonene in soil was dominated by aerobic microorganisms. A simple, rapid and effective gas chromatography–mass spectrometry method was developed for the simultaneous determination of d-limonene and its oxidation products in some vegetables and soils. Using the quick, easy, cheap, effective, rugged and safe (QuEChERS) method, the sample was extracted with n-hexane, purified with octadecylsilane (C18) and graphitized carbon black (GCB), and detected using gas chromatography-quadrupole mass spectrometry. The linear correlation coefficients of all analytes in the nine matrices were good (R 2 > 0.995). At levels of 50, 100, and 1000 μg kg −1 , the average recoveries ranged from 71.2 to 114.5%, while intra-day and inter-day precision were below 13.4%. The limits of detection (LODs) and the limits of quantification (LOQs) in all matrices for d-limonene and its five oxidation products were 1–16 and 4–48 μg kg −1 , respectively. The residual levels of d-limonene can be well described by first-order kinetics. Dissipation in soil was microbially dominated, with half-lives of 1.95–2.84 days in the three soils and no residue in tomatoes. Its oxidation products were converted in soil mainly by microorganisms, with more trans -isomer production compared to cis -isomer. Moreover, no d-limonene residue was detected in tomatoes, and the persistence of d-limonene in soil was limited. The results of this study can provide data to understand the fate of d-limonene in tomato and soil and for further study its suitability as an environmentally friendly agrochemical." @default.
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• W4224303429 date "2022-08-01" @default.
• W4224303429 modified "2023-10-01" @default.
• W4224303429 title "Development and validation of a method for determining d-limonene and its oxidation products in vegetables and soil using GC–MS" @default.
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• W4224303429 doi "https://doi.org/10.1016/j.microc.2022.107470" @default.
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