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- W4224983288 abstract "The purpose of this research is to investigate and identify polyphenolic complexes and other biologically active compounds by tandem mass spectrometry, presented in the leaves and stems of Ledum palustre L. Carbon dioxide, compressed to a supercritical state, was used for the most environmentally friendly extraction of polyphenolic complexes and other biologically active compounds of Ledum palustre L. The most effective extraction characteristics (pressure 350 bar; temperature 60 °С; extraction time 1-hour, co-solvent MeOH 3.5%) supercritical CO2-extraction of L. palustre were obtained empirically. To identify target analytes in supercritical extracts, High Performance Liquid Chromatography (HPLC) was used in combination with a BRUKER DALTONIKS ion trap. The results showed the presence of 61 biologically active compounds corresponding to the rhododendron species, of which 32 were identified for the first time in L. palustre. These are flavanols dihydrokaempferol, quercetin arabinoside, myricetin galactoside; flavones: diosmetin, nevadensin, cirsimaritin; flavanone naringenin; anthocyanins delphinidin, petunidin, cyanidin pentoside, delphinidin pentoside, peonidin 3-(6-O-acetyl) glucoside, peonidin-3-O-malonylglucoside, cyanidin-3-rutinoside, peonidin 3-O-glucoside; ellagic acid; lignan medioresinol; a type A procyanidin dimer; sterols fucosterol and avenasterol, etc." @default.
- W4224983288 created "2022-04-28" @default.
- W4224983288 creator A5012130040 @default.
- W4224983288 creator A5040981098 @default.
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- W4224983288 date "2022-03-10" @default.
- W4224983288 modified "2023-09-26" @default.
- W4224983288 title "INVESTIGATION OF SUPERCRITICAL CO2-EXTRACTS OF WILD LEDUM PALUSTRE L. (RHODODENDRON TO-MENTOSUM HARMAJA) AND IDENTIFICATION OF ITS METABOLITES BY TANDEM MASS SPECTROMETRY" @default.
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- W4224983288 doi "https://doi.org/10.14258/jcprm.2022019506" @default.
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