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• W4225152426 abstract "We have achieved the first anti-borylstannylation of alkynes by using (o-phenylenediaminato)borylstannanes. This reaction afforded 1-boryl-2-stannylalkenes with excellent regio- and stereoselectivity by a radical mechanism. This anti-addition manner is in sharp contrast to the syn-selectivity obtained during transition metal-catalyzed borylstannylation. The mild radical conditions enabled a broad substrate scope, and various types of aromatic and aliphatic alkynes were applicable. The origin of regio- and stereoselectivity was elucidated by DFT calculation of the reaction mechanism. The application of the borylstannylation products to cross- or homocoupling reactions provided ready access to either triarylethenes or bisborylbutadienes." @default.
• W4225152426 created "2022-05-01" @default.
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• W4225152426 date "2022-05-11" @default.
• W4225152426 modified "2023-10-16" @default.
• W4225152426 title "<i>anti</i> ‐Selective Borylstannylation of Alkynes with ( <i>o</i> ‐Phenylenediaminato)borylstannanes by a Radical Mechanism" @default.
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• W4225152426 doi "https://doi.org/10.1002/anie.202201883" @default.
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