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• W4229014018 startingPage "8248" @default.
• W4229014018 abstract "To overcome the challenge of synthesizing new and promising iron fluoride cathode materials, high-pressure synthesis was employed to obtain a new form of LiFe2F6 crystallized in the trigonal P321 α-LiMnFeF6 structure. Starting from solid fluorine sources, the trigonal structure was obtained for the first time for LiFe2F6 at 2.7 GPa, 500 °C, and characterized by synchrotron X-ray diffraction. Rietveld refinements revealed that a new form of LiFe2F6 possesses the Na2SiF6-type structure, which would provide enhanced Li+ diffusions. A Mössbauer spectrometry analysis was done with a paramagnetic structure obtained at 300 K and a magnetic sextet at 77 K with a 53 T hyperfine field for Fe3+ similarly to α-LiMnFeF6. The first electrochemistry tests indicate a good first cycle capacity of ∼150 mAh·g–1 with a charge process corresponding to Li+ disinsertion, a value doubled when compared to α-LiMnFeF6. These first experimental results show a new synthetic idea to discover materials designed for next generation batteries." @default.
• W4229014018 created "2022-05-08" @default.
• W4229014018 creator A5048872749 @default.
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• W4229014018 date "2022-05-06" @default.
• W4229014018 modified "2023-10-17" @default.
• W4229014018 title "High-Pressure Synthesis of Trigonal LiFe₂F₆: New Iron Fluoride with Li⁺ Tunnels as a Potential Cathode for Lithium-Ion Batteries" @default.
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• W4229014018 doi "https://doi.org/10.1021/acs.jpcc.2c01516" @default.
• W4229014018 hasPublicationYear "2022" @default.
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