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- W4229059454 endingPage "110217" @default.
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- W4229059454 abstract "Hydrogels with reactive thiourea functional groups were prepared by radiation-induced crosslinking of N-(Hydroxymethyl) acrylamide (HMA) and N-allyl thiourea (ATU) at different ATU content and irradiation doses. P(HMA-co-ATU) hydrogels were then utilized as template for in situ metal nanoparticle (MNP) preparation by the reduction of Ni2+, Co2+, and Cu2+ ions within the hydrogel matrix using sodium borohydride (NaBH4) as reducing agent. These [email protected](HMA-co-ATU) hydrogel composites (MNP = Co, Ni, and Cu) were further used as catalysts in the reduction reaction of 4-nitrophenol (4-NP) to 4-aminophenol (AP). Various parameters such as the effect of ATU content, the total dose used in the hydrogel preparation, MNPs type, and temperature on the catalytic activity of hydrogel composites were investigated. The activation energy, enthalpy, and entropy of [email protected](HMA-co-ATU) hydrogels for the reduction reaction of 4-NP to 4-AP were calculated as 42.5 kJ mol−1, 38.9 kJ mol−1, and −187.3 J mol−1 K−1, respectively." @default.
- W4229059454 created "2022-05-08" @default.
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- W4229059454 date "2022-09-01" @default.
- W4229059454 modified "2023-09-30" @default.
- W4229059454 title "P(HMA-co-ATU) hydrogel synthesis via gamma radiation and its use for in situ metal nanoparticle preparation and as catalyst in 4-nitrophenol reduction" @default.
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- W4229059454 doi "https://doi.org/10.1016/j.radphyschem.2022.110217" @default.
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