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• W4229082110 abstract "Nanoscale tailoring of catalytic materials and Li-battery alternatives has elevated the importance of in situ gas-phase electron microscopy. Such advanced techniques are often performed using an environmental cell inserted into a conventional S/TEM setup, as this method facilitates concurrent electrochemical and temperature stimulations in a convenient and cost-effective manner. However, these cells are made by encapsulating gas between two insulating membranes, which introduces additional electron scattering. We have evaluated strengths and limitations of the gas-phase E-cell S/TEM technique, both experimentally and through simulations, across a variety of practical parameters. We reveal the degradation of image quality in an E-cell setup from various components and explore opportunities to improve imaging quality through intelligent choice of experimental parameters. Our results underscore the benefits of using an E-cell STEM technique, due to its versatility and excellent ability to suppress the exotic contributions from the membrane device." @default.
• W4229082110 created "2022-05-08" @default.
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• W4229082110 date "2022-05-06" @default.
• W4229082110 modified "2023-10-14" @default.
• W4229082110 title "Effects of the Encapsulation Membrane in Operando Scanning Transmission Electron Microscopy" @default.
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• W4229082110 doi "https://doi.org/10.1021/acs.nanolett.2c00893" @default.
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