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• W4229448797 endingPage "133256" @default.
• W4229448797 startingPage "133256" @default.
• W4229448797 abstract "• Six adducts have been prepared and structurally characterized. • H-bonds have been illuminated. • Secondary interactions also have important role. • The synthons are analyzed. Cocrystallization of 6-methylpyridine-3-carboxamide, with mono- to dicarboxylic acids coformers afforded a total of six novel adducts including three co-crystals ( 2 , and 5 – 6 ) and two salts ( 1 , and 3 – 4 ). They have been featured by SCXRD, IR and EA, their m.p. were also measured. Their structural and supramolecular facets are fully inspected. The result tells that in all salts the aryl N in 6-methylpyridine-3-carboxamide is the only protonated position. The crystal packing is woven by the strong N H···O, O H···N and O H···O H-bonds. The CONH 2 dimers were made in 1 and 6 by a pair of N H···O H-bonds. Deep view of the crystal packing uncovered that different sets of subsidiary CH···O/CH 3 ···O, O···I, I···I, O···π, π···C, CH···π and π···π contacts contribute to the stabilization and expansion of the final 2D-3D structures. For the delicate balance of the various non-covalent bonds these structures contained homo/hetero supramolecular synthons or both, the common R 2 2 (8) graph set has been enclosed in all for the cooperation of H-bonds and non-covalent contacts." @default.
• W4229448797 created "2022-05-11" @default.
• W4229448797 creator A5004145168 @default.
• W4229448797 creator A5061485530 @default.
• W4229448797 creator A5062322488 @default.
• W4229448797 creator A5071026135 @default.
• W4229448797 date "2022-09-01" @default.
• W4229448797 modified "2023-10-02" @default.
• W4229448797 title "Noncovalent-bonded 2D-3D supramolecular adducts from 6-methylpyridine-3-carboxamide and carboxylic acids" @default.
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