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- W4229452019 endingPage "140507" @default.
- W4229452019 startingPage "140507" @default.
- W4229452019 abstract "The present work evaluates ethanol and glycerol electro-oxidation on Rh/C catalysts prepared using the Bromide Anion Exchange (BAE) method. Physicochemical characterizations were performed using Thermogravimetric Analysis (TGA), X-ray diffraction (XRD), and X-ray photoelectron spectroscopy (XPS). The SPAIRS investigations revealed that the CO adsorption modes on Rh sites occur on the linearly adsorbed CO (COL) and bridged bonded (COB) modes. In ethanol oxidation reaction (EOR), the Rh effect was evaluated by analyzing the products generated after bulk electrolysis using High-Performance Liquid Chromatography (HPLC) and in situ FTIR spectroscopy. The results confirmed the C-C cleavage Rh ability at low potentials and revealed that EOR follows both reaction pathways on Rh/C. While in glycerol oxidation reaction (GOR), Rh addition increases high added-value products formation such as glycerate ion. The GOR main route follows the glyceraldehyde pathway. The results highlighted that Rh is a good candidate for ethanol and glycerol electrochemical conversion at low potentials." @default.
- W4229452019 created "2022-05-11" @default.
- W4229452019 creator A5002175141 @default.
- W4229452019 creator A5009406696 @default.
- W4229452019 creator A5029724895 @default.
- W4229452019 creator A5053510468 @default.
- W4229452019 creator A5091609489 @default.
- W4229452019 date "2022-08-01" @default.
- W4229452019 modified "2023-10-16" @default.
- W4229452019 title "Insights on the C2 and C3 electroconversion in alkaline medium on Rh/C catalyst: in situ FTIR spectroscopic and chromatographic studies" @default.
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- W4229452019 doi "https://doi.org/10.1016/j.electacta.2022.140507" @default.