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- W4229488225 abstract "Abstract Despite recent advances, reactivity and site‐selectivity remain significant obstacles for the practical application of C(sp 3 )−H bond functionalization methods. Here, we describe a system that combines a salicylic‐aldehyde‐derived L,X‐type directing group with an electron‐deficient 2‐pyridone ligand to enable the β‐methylene C(sp 3 )−H arylation of aliphatic alcohols, which has not been possible previously. Notably, this protocol is compatible with heterocycles embedded in both alcohol substrates and aryl coupling partners. A site‐ and stereo‐specific annulation of dihydrocholesterol and the synthesis of a key intermediate of englitazone illustrate the practicality of this method." @default.
- W4229488225 created "2022-05-11" @default.
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- W4229488225 date "2020-03-11" @default.
- W4229488225 modified "2023-10-16" @default.
- W4229488225 title "Ligand‐Enabled β‐Methylene C(sp <sup>3</sup> )−H Arylation of Masked Aliphatic Alcohols" @default.
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- W4229488225 doi "https://doi.org/10.1002/ange.202000632" @default.
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