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- W4229494236 abstract "Etching of gold with an excess of thiol ligand is used in both synthesis and analysis of gold particles. Mechanistically, the process of etching gold with excess thiol is unclear. Previous studies have obliquely considered the role of oxygen in thiolate etching of gold. Herein, we show that oxygen or a radical initiator is a necessary component for efficient etching of gold by thiolates. Attenuation of the etching process by radical scavengers in the presence of oxygen, and the restoration of activity by radical initiators under inert atmosphere, strongly implicate the oxygen radical. These data led us to propose an atomistic mechanism in which the oxygen radical initiates the etching process." @default.
- W4229494236 created "2022-05-11" @default.
- W4229494236 creator A5007065972 @default.
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- W4229494236 date "2015-06-18" @default.
- W4229494236 modified "2023-09-26" @default.
- W4229494236 title "Radicals Are Required for Thiol Etching of Gold Particles" @default.
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- W4229494236 doi "https://doi.org/10.1002/ange.201502934" @default.
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