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- W4230394013 abstract "The aim of this article was to develop a chemometric methodology for determining the chemical profile of cocaine samples seized in Minas Gerais State, Brazil. The adulterant detection and the cocaine determination were performed by gas chromatography-mass spectrometry (GC-MS). Spectra of 91 samples were obtained by attenuated total reflection Fourier transform infrared spectroscopy (ATR-FTIR) and used to build an exploratory principal component analysis (PCA) model. The first principal component (PC1) discriminated samples of more purity from the more diluted/adulterated ones, which were characterized by the presence of lidocaine, caffeine and benzocaine. PC2 discriminated the two chemical forms of cocaine, hydrochloride and base. In addition, two supervised discriminant partial least-squares models (partial least-squares discriminant analysis, PLS-DA) were developed for classifying the samples according to dilution (above and below 15% m/m) and chemical form, with a rate of success that varied between 83 and 97%. The classification models constitute a simple, rapid and non-destructive tool, of great value for both forensic experts and criminal investigators." @default.
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- W4230394013 date "2013-03-01" @default.
- W4230394013 modified "2023-10-14" @default.
- W4230394013 title "Analysis of seized cocaine samples by using chemometric methods and FTIR spectroscopy" @default.
- W4230394013 doi "https://doi.org/10.1590/s0103-50532013000300019" @default.
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