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• W4231146682 abstract "The synthesis of Segment B/C corresponding to the C26 through to the C1 positions of tautomycin was achieved by coupling between Segment B (an epoxide) and Segment C (a sulfone carbanion) in the presence of boron trifluoride etherate (BF3·OEt2). Two routes have been developed in esterification of Segment A with Segment B/C. The first route employed Segment A with furan moiety as masked maleic anhydride. In the second route, maleic anhydride as Segment A was directly used to accomplish the improved synthesis. Removal of the silyl protecting group with pyridinium poly(hydrogen fluoride) (HF-Py) at the final step completed the total synthesis of tautomycin." @default.
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• W4231146682 date "1997-04-01" @default.
• W4231146682 modified "2023-10-09" @default.
• W4231146682 title "Total synthesis of (+)-tautomycin" @default.
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• W4231146682 doi "https://doi.org/10.1016/s0040-4020(97)00230-5" @default.
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