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- W4235583886 abstract "Abstract A new process for elaborating continuously organic-inorganic hybrid materials by reactive extrusion is presented. This synthesis consists in formulating a copolymer of ethylene and vinyl acetate (EVA)/tetrapropoxysilane (TPOS or Si(OC 3 H 7 ) 4 )/catalyst blend by a corotating twin screw extruder followed by two successive reaction steps: on line microwave crosslinking reaction and hydrolysis-condensation reactions leading to a silica network cografted onto the organic matrix. Extrusion feed rate (Q), temperature, microwave oven power (P), and microwave curing time (t mw ) were studied. Crosslinking density was evaluated before and after hydrolysis-condensation reactions and compared with the previous results obtained in static conditions. These materials tailored by an on line process present a permanent elasticity at high temperature (up to 200 °C) and a certain optical transparency. This new approach offers the possibility to synthesize massive samples based on organic-inorganic hybrid material." @default.
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- W4235583886 date "2005-08-01" @default.
- W4235583886 modified "2023-10-14" @default.
- W4235583886 title "Organic-Inorganic Hybrid Material Synthesis by on Line Coupling Twin Screw Extruder with a Microwave Oven" @default.
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- W4235583886 doi "https://doi.org/10.1515/ipp-2005-0062" @default.
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